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Both the heat transfer coefficient and the effective heating surface. When NCG
Are present, the evaporators require continuous venting from the steam side. The
NCG are odorous and may be inflammable. Kraft NCG are typically forwarded to
Incineration, whereas sulphite NCG can be re-used for cooking acid preparation.
Evaporators are usually arranged in groups in order to improve the steam economy,
And to accommodate the large heat exchange surfaces. When black liquor is
Transferred from one evaporator body to the other, the thickened liquor may be
Separately extracted from the evaporator sump (see Fig. 9.4), or branched off after
The circulation liquor pump. The separate extraction of thick liquor before
Recovery
Droplet separator
CIRCULATION
LIQUOR
STEAM
CONDENSATE
VAPOUR
Liquor distribution
Heating elements
THIN LIQUOR
THICK LIQUOR
NCG VENT
Fig. 9.4 Example of a plate-type falling film evaporator.
Dilution with thin liquor keeps the concentration level in the evaporator comparatively
Low. This is especially helpful at high dry solids concentrations, where the
Boiling point rise can considerably reduce the evaporator performance.
The performance of an evaporator is determined by the heat transfer rate, Q
(W). The very basic equation of heat transfer relates the transfer rate to the overall
heat transfer coefficient, U (W m–2 K–1), the surface of the heating elements, A
(m2), and the effective temperature difference, DTeff (°C):
Q _ UADTeff _9_
The effective temperature difference which drives the evaporation is given by
The difference between the steam side condensing temperature and the vapor side
gas temperature, DT, minus the boiling point rise, BPR:
DTeff _ DT _ BPR _10_
The overall heat transfer coefficient U depends on evaporator design, on the
Physical properties of the liquor (especially its dry solids concentration and viscosity),
And on potential fouling of heat exchange surfaces. Typical heat transfer coefficients
for falling film evaporators are between 700 and 2000 Wm–2 K–1, with lowend
Values related to high dry solids concentrations. The heat transfer rate is pro-
Chemical Recovery Processes
Portional to the evaporation capacity. Thus, more surface area and a higher temperature
Difference result in increased capacity.
As concentrations rise during evaporation, fouling of the heat exchanger surfaces
On the liquor side can be caused by the precipitation of inorganic and organics
Liquor compounds. Inorganics with a tendency to scaling include calcium carbonate,
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Solids concentration in the black liquor for the purpose of firing the thick liquor | | | Sodium salts, gypsum, silicates, or oxalates. Scaling worsens with higher |