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Several parameters have been suggested over time to describe the ratio of liquor
flows around a washer. The single most relevant parameter – which has also managed
to find its way into practical application – is the dilution factor.
Imagine a pulp washer as a black box with the flows entering and leaving, as
shown in Fig. 5.17. Depending on the feed consistency N in, a certain amount of
liquor L in enters the washer with the pulp P. At the same time, a certain amount
of liquor L out leaves the washer with the pulp at the outlet consistency N out. Wash
liquor in the amount of WL is used for washing, and the filtrate quantity F is generated.
Washer
Pulp feed
P, Nin, Lin
Pulp discharge
P, Nout, Lout
Filtrate
F
Wash liquor
WL
Fig. 5.17 Streams around a pulp washer.
The dilution factor is defined as the difference of wash liquor flow and liquor
flow leaving with the washed pulp, related to the pulp flow:
DF __
WL _ Lout
P _16_
where DF = dilution factor (t odt–1); WL = flow rate of wash liquor (t h–1); L out = flow
rate of liquor accompanying the discharged pulp (t h–1);and P = flow rate of pulp
(odt h–1).
In practice, the dilution factor is often expressed in volumetric terms (m3 t–1)
rather than as a mass ratio (t t–1). Here, we will continue to use the mass ratio, as
in this way the process engineer’s calculations are simplified. (When we return to
the field, it may sometimes be acceptable simply to substitute the mass ratio by
the volumetric term due to the small error made compared to the variability of
erratic mill data.)
The liquor flow L out can be calculated from the discharge consistency N out and
pulp production capacity P:
Lout _ P
_ Nout _ 1_ _17_
thereby providing another useful formula for the dilution factor:
DF _
WL
P _
Nout _ 1 _18_
So, why is this parameter called the dilution factor? Let us examine the overall
mass balance around the washer:
Lin _ WL _ Lout _ F _ 0 _19_
530 5 Pulp Washing
In another form, this equation reads:
WL _ Lout _ F _ Lin _20_
The left-hand term represents the numerator of Eq. (16). If the quantity of wash
liquor WL is equal to the liquor quantity leaving with the discharged pulp L out, the
filtrate volume F equals the liquor volume in the pulp feed L in. There is no dilution
of the filtrate and the dilution factor is zero.
Any wash liquor charge which increases the amount of filtrate above the
amount of liquor in the pulp feed will dilute the filtrate. In this case, the dilution
factor is positive. Any wash liquor charge which reduces the amount of filtrate
below the amount of liquor in the pulp feed will also reduce the amount of filtrate.
Then, the dilution factor is negative.
When the dilution factor of displacement washing is negative, a portion of the
contaminated liquor stays with the pulp and leaves the washer as carry-over. It is
apparent that a washing stage can reach high efficiency only at positive dilution
factors.
There is a clear correlation of washing efficiency and dilution factor in a way,
that the washing efficiency improves with higher dilution factors. There is, however,
a ceiling for the washing efficiency which is correlated to the physical limits
of liquor penetration through the pulp mat.
Regardless of its undisputable beneficial effect on washing efficiency, it is
important to note that a high positive dilution factor can substantially affect downstream
mill areas. In the case of brownstock washing, an increased dilution factor
means additional evaporation requirements;in the case of washing in the bleach
plant, the increased filtrate flow places a challenge on the hydraulic capacity of the
biological treatment plant or of the alternative filtrate purification system, respectively.
For a particular application, the favorable range of dilution factors is dependent
upon the type and specific design of the washing equipment. As a rule of thumb,
drum and belt washers are typically operated at dilution factors of 1–3 t odt–1,
while wash presses usually perform best at dilution factors of 2–4 t odt–1.
In a multi-stage washing system, it is most important to note that all washers in
the system must be operated at the same dilution factor in order to avoid overflows
or shortage of filtrate between the stages. The dilution factor of a multi-stage
system is therefore set by controlling the flow to the last washing stage.
5.4 Washing Parameters 531
532 5 Pulp Washing
Example: Calculation of wash liquor quantities in a closed, countercurrent,
two-stage washing system
The pulp production capacity, the outlet consistencies of the two washers,
and the desired dilution factor are known:
Pulp production capacity, P = 25 odt h–1
Washer no. 1 discharge consistency, N1,out = 11%
Washer no. 2 discharge consistency, N2,out = 15%
Dilution factor, DF = 2.0 t odt–1
In order to determine the wash liquor quantities, we first calculate the
amounts of liquor leaving the washers with the pulp:
L 1_ out _ P
N 1_ out _ _ 1__ 25
_0_ 11 _ 1__ 202 t h_1
L 2_ out _ P
N 2_ out _ _ 1__ 25
_0_ 15 _ 1__ 142 t h_1
Then, the wash liquor flow rate to the first washer amounts to
WL 1 _ L 1_ out _ DF _ P _ 202 _ 2_ 0 _ 25 _ 252 t h_1
and the wash liquor flow rate to the second washer is
WL 2 _ L 2_ out _ DF _ P _ 142 _ 2_ 0 _ 25 _ 192 t h_1
Note that in a closed countercurrent washing system, the first washer
must be operated with a much higher wash liquor quantity than the second
washer, simply because its discharge consistency is lower.
5.4.3
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